TA Instruments

AR1707-0001f

04/09/2012 16:34:52

Sample name	ASW 10 mm from base, 60 mm to top, disk 7 PMMA fouled
Sample notes	 
Experiment notes	Plastic parallel plate with adaptor supplied by Southampton Uni., on ETC rod with grub screws.

Distances fromlower surface of PP plate. Southampton container.
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1707
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	04/09/2012 16:34:52

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:01:00 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	3.100 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.262 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	3
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	18.42 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

-13.70	7.479	-1.833	1.0040	22.4	610.9	5.2495	10000	0.1499	10.92	6.5618	656.18	3.383E-3	0.0	1.0	61.004	-42.046	5.983
1.027	14.15	0.07261	2.0120	22.4	596.8	16.1993	10000	0.1465	2.981	20.249	2024.9	3.384E-3	0.0	1.0	62.012	3.1523	11.32
1.806	20.36	0.08870	3.0200	22.4	603.5	29.4752	10000	0.1481	1.455	36.844	3684.4	3.384E-3	0.1	1.1	63.020	5.5413	16.29
2.452	23.86	0.1027	4.0040	22.4	615.0	43.2926	10000	0.1510	1.080	54.116	5411.6	3.384E-3	0.1	1.1	64.004	7.5215	19.09
3.773	31.43	0.1200	5.0200	22.4	599.3	69.9093	10000	0.1471	0.6067	87.387	8738.7	3.384E-3	0.1	1.1	65.020	11.574	25.14
5.150	37.32	0.1380	6.0120	22.4	616.7	95.9699	10000	0.1514	0.4427	119.96	11996	3.383E-3	0.1	1.1	66.012	15.800	29.86
6.494	42.93	0.1513	7.0040	22.4	595.2	128.5170	10000	0.1461	0.3229	160.65	16065	3.384E-3	0.1	1.1	67.004	19.923	34.35
8.177	49.47	0.1653	8.0200	22.4	598.5	167.4610	10000	0.1469	0.2445	209.33	20933	3.384E-3	0.1	1.1	68.020	25.086	39.58
10.69	57.83	0.1849	9.0040	22.4	595.2	225.6150	10000	0.1461	0.1780	282.02	28202	3.384E-3	0.2	1.2	69.004	32.803	46.27
12.54	63.95	0.1961	10.012	22.4	588.6	277.5630	10000	0.1445	0.1439	346.95	34695	3.383E-3	0.2	1.2	70.012	38.475	51.16
14.58	69.88	0.2086	11.016	22.4	584.4	328.1430	10000	0.1434	0.1197	410.18	41018	3.383E-3	0.2	1.2	71.016	44.732	55.90
16.62	75.33	0.2207	12.000	22.4	584.4	379.3010	10000	0.1434	0.1030	474.13	47413	3.384E-3	0.2	1.2	72.000	51.003	60.27
18.61	80.71	0.2305	13.020	22.4	586.1	437.1890	10000	0.1438	0.08997	546.49	54649	3.383E-3	0.2	1.2	73.020	57.084	64.57
21.10	86.62	0.2436	14.032	22.4	579.5	500.7050	10000	0.1422	0.07724	625.88	62588	3.383E-3	0.2	1.2	74.032	64.737	69.29
24.09	94.77	0.2542	15.016	22.4	579.5	596.2710	10000	0.1422	0.06452	745.34	74534	3.384E-3	0.3	1.3	75.016	73.895	75.82
26.67	100.1	0.2665	16.004	22.4	567.1	666.3340	10000	0.1392	0.05663	832.92	83292	3.383E-3	0.3	1.3	76.004	81.822	80.06
28.97	105.8	0.2738	17.020	22.4	577.8	742.6990	10000	0.1418	0.05161	928.37	92837	3.384E-3	0.3	1.3	77.020	88.877	84.65
32.39	113.9	0.2844	18.024	22.4	566.3	857.1610	10000	0.1390	0.04367	1071.5	1.0715E5	3.384E-3	0.3	1.3	78.024	99.364	91.10
34.83	118.9	0.2929	19.000	22.4	561.3	933.2900	10000	0.1378	0.03968	1166.6	1.1666E5	3.384E-3	0.3	1.3	79.000	106.86	95.15
37.47	124.4	0.3012	20.016	22.4	564.6	1022.2500	10000	0.1386	0.03649	1277.8	1.2778E5	3.383E-3	0.3	1.3	80.016	114.95	99.51
41.58	132.4	0.3140	21.028	22.4	561.3	1156.4500	10000	0.1378	0.03202	1445.6	1.4456E5	3.384E-3	0.4	1.4	81.028	127.55	105.9
44.14	137.5	0.3210	22.020	22.4	558.0	1244.2300	10000	0.1370	0.02952	1555.3	1.5553E5	3.384E-3	0.4	1.4	82.020	135.42	110.0
47.52	142.9	0.3325	23.000	22.4	536.5	1345.7000	10000	0.1317	0.02627	1682.1	1.6821E5	3.384E-3	0.4	1.4	83.000	145.79	114.3
51.58	150.9	0.3418	24.020	22.4	544.8	1499.2900	10000	0.1337	0.02392	1874.1	1.8741E5	3.384E-3	0.4	1.4	84.020	158.24	120.7
54.01	156.0	0.3462	25.024	22.4	540.6	1599.1200	10000	0.1327	0.02221	1998.9	1.9989E5	3.384E-3	0.4	1.4	85.024	165.71	124.8
57.05	161.4	0.3534	26.004	22.4	540.6	1713.1000	10000	0.1327	0.02075	2141.4	2.1414E5	3.384E-3	0.4	1.4	86.004	175.02	129.1
62.43	169.4	0.3685	27.012	22.4	525.8	1885.2500	10000	0.1290	0.01832	2356.6	2.3566E5	3.384E-3	0.5	1.5	87.012	191.53	135.5
65.32	174.5	0.3743	28.016	22.4	529.9	1997.9100	10000	0.1301	0.01739	2497.4	2.4974E5	3.384E-3	0.5	1.5	88.016	200.41	139.6
68.36	179.6	0.3805	29.020	22.4	526.6	2118.1001	10000	0.1292	0.01632	2647.6	2.6476E5	3.384E-3	0.5	1.5	89.020	209.72	143.7
74.00	187.6	0.3944	30.028	22.4	525.8	2308.6599	10000	0.1290	0.01493	2885.8	2.8858E5	3.384E-3	0.5	1.5	90.028	227.03	150.1
76.71	192.8	0.3979	31.008	22.4	510.9	2434.3999	10000	0.1254	0.01375	3043.0	3.0430E5	3.384E-3	0.5	1.5	91.008	235.34	154.2
82.50	200.6	0.4113	32.132	22.4	506.7	2636.7100	10000	0.1244	0.01259	3295.9	3.2959E5	3.383E-3	0.5	1.5	92.132	253.12	160.5
85.73	205.9	0.4164	33.024	22.4	504.3	2776.4700	10000	0.1238	0.01189	3470.6	3.4706E5	3.384E-3	0.6	1.6	93.024	263.02	164.7
89.21	211.1	0.4227	34.016	22.4	505.9	2914.8501	10000	0.1242	0.01136	3643.6	3.6436E5	3.384E-3	0.6	1.6	94.016	273.69	168.8
94.38	218.7	0.4316	35.080	22.4	494.3	3129.6499	10000	0.1213	0.01034	3912.1	3.9121E5	3.383E-3	0.6	1.6	95.080	289.56	174.9
97.65	224.0	0.4360	36.020	22.4	496.8	3281.3401	10000	0.1219	9.903E-3	4101.7	4.1017E5	3.384E-3	0.6	1.6	96.020	299.58	179.2
102.2	229.2	0.4459	37.004	22.4	487.7	3432.8301	10000	0.1197	9.288E-3	4291.0	4.2910E5	3.384E-3	0.6	1.6	97.004	313.46	183.3
107.1	236.7	0.4524	38.004	22.4	492.7	3661.8501	10000	0.1209	8.794E-3	4577.3	4.5773E5	3.384E-3	0.6	1.6	98.004	328.53	189.4
111.0	241.9	0.4587	39.004	22.4	488.6	3825.9900	10000	0.1199	8.350E-3	4782.5	4.7825E5	3.383E-3	0.7	1.7	99.004	340.41	193.5
117.6	249.6	0.4711	40.024	22.4	480.3	4072.6899	10000	0.1179	7.707E-3	5090.9	5.0909E5	3.384E-3	0.7	1.7	100.024	360.84	199.7
121.3	254.7	0.4764	41.004	22.4	446.4	4234.7998	10000	0.1096	6.882E-3	5293.5	5.2935E5	3.384E-3	0.7	1.7	101.004	372.20	203.7
124.0	262.5	0.4722	42.020	22.4	463.8	4502.7002	10000	0.1138	6.729E-3	5628.4	5.6284E5	3.384E-3	0.7	1.7	102.020	380.28	210.0
130.7	267.7	0.4883	43.020	22.4	443.1	4676.6001	10000	0.1088	6.184E-3	5845.8	5.8458E5	3.384E-3	0.7	1.7	103.020	400.99	214.1
135.3	272.7	0.4961	44.024	22.4	446.4	4853.3999	10000	0.1096	6.002E-3	6066.8	6.0668E5	3.384E-3	0.7	1.7	104.024	415.05	218.2
140.3	280.4	0.5005	45.004	22.4	436.5	5134.5400	10000	0.1071	5.551E-3	6418.2	6.4182E5	3.384E-3	0.8	1.8	105.004	430.58	224.3
144.8	285.6	0.5069	46.024	22.4	458.8	5321.2500	10000	0.1126	5.626E-3	6651.6	6.6516E5	3.384E-3	0.8	1.8	106.024	444.14	228.5
151.3	293.2	0.5160	47.020	22.4	440.6	5604.2300	10000	0.1081	5.127E-3	7005.3	7.0053E5	3.384E-3	0.8	1.8	107.020	464.10	234.5
157.0	298.2	0.5265	48.016	22.4	426.6	5799.7300	10000	0.1047	4.797E-3	7249.7	7.2497E5	3.384E-3	0.8	1.8	108.016	481.65	238.6
158.9	303.4	0.5237	49.004	22.4	441.4	6001.5000	10000	0.1083	4.796E-3	7501.9	7.5019E5	3.384E-3	0.8	1.8	109.004	487.41	242.7
166.7	311.0	0.5361	50.004	22.4	405.1	6304.5000	10000	0.09942	4.187E-3	7880.6	7.8806E5	3.384E-3	0.8	1.8	110.004	511.50	248.8
170.2	316.1	0.5385	51.020	22.4	406.7	6512.9102	10000	0.09982	4.071E-3	8141.1	8.1411E5	3.384E-3	0.9	1.9	111.020	522.16	252.9
176.2	323.8	0.5441	52.004	22.4	417.5	6834.1201	10000	0.1025	3.981E-3	8542.7	8.5427E5	3.384E-3	0.9	1.9	112.004	540.56	259.1
180.7	328.9	0.5493	53.004	22.4	406.7	7050.8398	10000	0.09982	3.759E-3	8813.6	8.8136E5	3.383E-3	0.9	1.9	113.004	554.29	263.1
187.5	336.5	0.5574	54.004	22.4	398.4	7376.6001	10000	0.09779	3.520E-3	9220.8	9.2208E5	3.383E-3	0.9	1.9	114.004	575.35	269.2
190.1	341.6	0.5564	55.004	22.4	393.5	7603.4800	10000	0.09658	3.371E-3	9504.4	9.5044E5	3.384E-3	0.9	1.9	115.004	583.19	273.3
198.5	346.7	0.5725	56.004	22.4	364.6	7830.2998	10000	0.08947	3.032E-3	9787.9	9.7879E5	3.383E-3	0.9	1.9	116.004	609.02	277.4
206.4	354.3	0.5827	57.016	22.4	388.5	8171.8501	10000	0.09536	3.096E-3	10215	1.0215E6	3.384E-3	1.0	2.0	117.016	633.31	283.4
211.0	359.4	0.5872	58.004	22.4	369.5	8410.2900	10000	0.09069	2.861E-3	10513	1.0513E6	3.384E-3	1.0	2.0	118.004	647.41	287.5
216.6	367.0	0.5902	59.004	22.4	377.8	8769.6797	10000	0.09272	2.804E-3	10962	1.0962E6	3.383E-3	1.0	2.0	119.004	664.54	293.6
221.7	372.0	0.5959	60.020	22.4	352.2	9009.2695	10000	0.08643	2.544E-3	11262	1.1262E6	3.384E-3	1.0	2.0	120.020	680.16	297.6

Peak hold step

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

226.5	375.0	0.6040	1.0000	22.4	351.3	274.4310	10000	0.08623	2.498E-3	343.04	34304	3.383E-3	0.0	2.0	122.000	694.89	300.0
224.4	375.0	0.5983	1.9920	22.4	363.7	528.0010	10000	0.08927	2.587E-3	660.00	66000	3.384E-3	0.0	2.0	122.992	688.37	300.0
226.0	375.0	0.6027	2.9920	22.4	342.2	902.5730	10000	0.08400	2.434E-3	1128.2	1.1282E5	3.383E-3	0.0	2.1	123.992	693.37	300.0
226.7	375.0	0.6045	3.9920	22.4	329.8	1157.9500	10000	0.08095	2.345E-3	1447.4	1.4474E5	3.384E-3	0.1	2.1	124.992	695.49	300.0
224.5	375.0	0.5987	4.9960	22.4	351.3	1405.2700	10000	0.08623	2.498E-3	1756.6	1.7566E5	3.384E-3	0.1	2.1	125.996	688.78	300.0
224.7	375.0	0.5991	5.9920	22.4	344.7	1782.4900	10000	0.08461	2.451E-3	2228.1	2.2281E5	3.384E-3	0.1	2.1	126.992	689.30	300.0
225.8	375.0	0.6022	6.9960	22.4	335.6	2037.0601	10000	0.08237	2.386E-3	2546.3	2.5463E5	3.384E-3	0.1	2.1	127.996	692.83	300.0
227.2	375.0	0.6059	7.9920	22.4	340.6	2410.9600	10000	0.08359	2.422E-3	3013.7	3.0137E5	3.384E-3	0.1	2.1	128.992	697.07	300.0
226.6	375.0	0.6042	8.9920	22.4	351.3	2661.9800	10000	0.08623	2.498E-3	3327.5	3.3275E5	3.383E-3	0.1	2.2	129.992	695.09	300.0
225.5	375.0	0.6013	9.9960	22.4	345.5	2915.6201	10000	0.08481	2.457E-3	3644.5	3.6445E5	3.384E-3	0.2	2.2	130.996	691.85	300.0
225.9	375.0	0.6024	10.992	22.4	331.5	3292.8401	10000	0.08136	2.357E-3	4116.1	4.1161E5	3.384E-3	0.2	2.2	131.992	693.03	300.0
228.3	375.0	0.6087	12.008	22.4	307.5	3545.7000	10000	0.07548	2.187E-3	4432.1	4.4321E5	3.384E-3	0.2	2.2	133.008	700.28	300.0
224.6	375.0	0.5991	12.996	22.4	361.2	3922.0801	10000	0.08866	2.569E-3	4902.6	4.9026E5	3.384E-3	0.2	2.2	133.996	689.21	300.0
225.3	375.0	0.6008	13.992	22.4	358.8	4173.8301	10000	0.08805	2.551E-3	5217.3	5.2173E5	3.384E-3	0.2	2.2	134.992	691.17	300.0
227.4	375.0	0.6063	14.996	22.4	352.2	4423.0400	10000	0.08643	2.504E-3	5528.8	5.5288E5	3.384E-3	0.2	2.3	135.996	697.55	300.0
226.8	375.0	0.6049	15.996	22.4	360.4	4801.5400	10000	0.08846	2.563E-3	6001.9	6.0019E5	3.384E-3	0.3	2.3	136.996	695.91	300.0
225.5	375.0	0.6013	16.996	22.4	373.6	5049.5000	10000	0.09171	2.657E-3	6311.9	6.3119E5	3.383E-3	0.3	2.3	137.996	691.79	300.0
224.3	375.0	0.5980	18.012	22.4	332.3	5429.0298	10000	0.08156	2.363E-3	6786.3	6.7863E5	3.384E-3	0.3	2.3	139.012	688.05	300.0
224.8	375.0	0.5995	18.996	22.4	338.9	5677.8599	10000	0.08319	2.410E-3	7097.3	7.0973E5	3.384E-3	0.3	2.3	139.996	689.75	300.0
225.1	375.0	0.6002	19.992	22.4	332.3	5929.1899	10000	0.08156	2.363E-3	7411.5	7.4115E5	3.383E-3	0.3	2.3	140.992	690.51	300.0
223.4	375.0	0.5957	21.008	22.4	343.9	6306.2598	10000	0.08440	2.445E-3	7882.8	7.8828E5	3.383E-3	0.4	2.4	142.008	685.38	300.0
226.3	375.0	0.6034	22.012	22.4	372.0	6557.5298	10000	0.09130	2.645E-3	8196.9	8.1969E5	3.383E-3	0.4	2.4	143.012	694.25	300.0
224.6	375.0	0.5989	22.992	22.4	386.0	6808.9502	10000	0.09475	2.745E-3	8511.2	8.5112E5	3.383E-3	0.4	2.4	143.992	689.08	300.0
226.5	375.0	0.6040	24.020	22.4	338.9	7185.9502	10000	0.08319	2.410E-3	8982.4	8.9824E5	3.383E-3	0.4	2.4	145.020	694.94	300.0
224.0	375.0	0.5974	25.012	22.4	327.4	7437.2598	10000	0.08034	2.328E-3	9296.6	9.2966E5	3.384E-3	0.4	2.4	146.012	687.27	300.0
224.5	375.0	0.5988	25.996	22.4	391.8	7816.6401	10000	0.09617	2.786E-3	9770.8	9.7708E5	3.383E-3	0.4	2.4	146.996	688.89	300.0
224.4	375.0	0.5984	27.004	22.4	342.2	8065.5801	10000	0.08400	2.434E-3	10082	1.0082E6	3.384E-3	0.5	2.5	148.004	688.45	300.0
221.8	375.0	0.5915	27.996	22.4	379.4	8316.7305	10000	0.09313	2.698E-3	10396	1.0396E6	3.383E-3	0.5	2.5	148.996	680.52	300.0
226.5	375.0	0.6041	29.012	22.4	349.7	8693.9697	10000	0.08582	2.487E-3	10867	1.0867E6	3.383E-3	0.5	2.5	150.012	695.02	300.0
223.1	375.0	0.5950	29.996	22.4	368.7	8945.8799	10000	0.09049	2.622E-3	11182	1.1182E6	3.383E-3	0.5	2.5	150.996	684.60	300.0

Continuous ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

223.2	370.8	0.6019	1.0120	22.4	327.4	283.7500	10000	0.08034	2.381E-3	354.69	35469	3.383E-3	0.0	2.5	152.012	684.71	296.6
216.1	365.8	0.5907	2.0080	22.4	347.2	522.6380	10000	0.08521	2.595E-3	653.30	65330	3.384E-3	0.0	2.6	153.008	662.89	292.6
209.2	358.1	0.5842	3.0200	22.4	375.3	879.3080	10000	0.09211	2.926E-3	1099.1	1.0991E5	3.384E-3	0.1	2.6	154.020	641.91	286.5
204.0	353.0	0.5780	4.0080	22.4	377.0	1116.9600	10000	0.09252	3.026E-3	1396.2	1.3962E5	3.383E-3	0.1	2.6	155.008	625.87	282.4
196.6	345.4	0.5692	5.0080	22.4	353.0	1457.3199	10000	0.08663	2.959E-3	1821.7	1.8217E5	3.383E-3	0.1	2.6	156.008	603.19	276.3
190.0	340.3	0.5582	6.0040	22.4	388.5	1680.4200	10000	0.09536	3.355E-3	2100.5	2.1005E5	3.383E-3	0.1	2.6	157.004	582.77	272.3
184.0	335.2	0.5491	7.0200	22.4	407.5	1905.8700	10000	0.1000	3.628E-3	2382.3	2.3823E5	3.384E-3	0.1	2.6	158.020	564.60	268.1
177.4	327.6	0.5413	8.0080	22.4	422.4	2225.0400	10000	0.1037	3.935E-3	2781.3	2.7813E5	3.383E-3	0.1	2.7	159.008	544.14	262.1
173.8	322.6	0.5390	9.0080	22.4	417.5	2437.8701	10000	0.1025	4.012E-3	3047.3	3.0473E5	3.383E-3	0.2	2.7	160.008	533.36	258.1
166.9	314.8	0.5300	10.004	22.4	444.7	2760.7300	10000	0.1092	4.487E-3	3450.9	3.4509E5	3.383E-3	0.2	2.7	161.004	511.93	251.9
164.0	309.8	0.5295	11.004	22.4	419.9	2957.4299	10000	0.1031	4.376E-3	3696.8	3.6968E5	3.384E-3	0.2	2.7	162.004	503.28	247.8
155.0	302.2	0.5128	12.020	22.4	436.5	3257.8701	10000	0.1071	4.780E-3	4072.3	4.0723E5	3.383E-3	0.2	2.7	163.020	475.43	241.8
152.5	297.0	0.5134	13.004	22.4	416.6	3458.1101	10000	0.1023	4.723E-3	4322.6	4.3226E5	3.383E-3	0.2	2.7	164.004	467.79	237.6
148.3	291.8	0.5083	14.004	22.4	415.8	3652.6699	10000	0.1021	4.882E-3	4565.8	4.5658E5	3.383E-3	0.2	2.8	165.004	455.08	233.5
140.7	284.3	0.4949	15.004	22.4	421.6	3935.4800	10000	0.1035	5.217E-3	4919.4	4.9194E5	3.383E-3	0.3	2.8	166.004	431.63	227.4
138.3	279.1	0.4953	16.020	22.4	458.8	4123.0601	10000	0.1126	5.889E-3	5153.8	5.1538E5	3.383E-3	0.3	2.8	167.020	424.16	223.3
132.5	271.3	0.4886	17.004	22.4	446.4	4398.2998	10000	0.1096	6.065E-3	5497.9	5.4979E5	3.384E-3	0.3	2.8	168.004	406.64	217.0
127.4	266.3	0.4784	18.004	22.4	470.4	4571.7202	10000	0.1154	6.634E-3	5714.7	5.7147E5	3.383E-3	0.3	2.8	169.004	390.83	213.0
123.1	261.1	0.4713	19.016	22.4	463.8	4746.7998	10000	0.1138	6.802E-3	5933.5	5.9335E5	3.383E-3	0.3	2.8	170.016	377.53	208.9
116.5	253.3	0.4598	20.004	22.4	482.8	5005.7500	10000	0.1185	7.523E-3	6257.2	6.2572E5	3.384E-3	0.3	2.9	171.004	357.36	202.7
113.5	248.3	0.4572	21.020	22.4	465.4	5165.7900	10000	0.1142	7.549E-3	6457.2	6.4572E5	3.383E-3	0.4	2.9	172.020	348.26	198.6
109.4	240.6	0.4547	22.020	22.4	471.2	5409.7402	10000	0.1156	8.141E-3	6762.2	6.7622E5	3.383E-3	0.4	2.9	173.020	335.59	192.5
104.1	235.3	0.4422	23.020	22.4	498.5	5572.0801	10000	0.1223	9.003E-3	6965.1	6.9651E5	3.383E-3	0.4	2.9	174.020	319.26	188.2
97.89	227.7	0.4300	24.028	22.4	502.6	5797.2100	10000	0.1234	9.696E-3	7246.5	7.2465E5	3.383E-3	0.4	2.9	175.028	300.32	182.1
95.19	222.5	0.4278	25.024	22.4	486.1	5947.1602	10000	0.1193	9.817E-3	7434.0	7.4340E5	3.384E-3	0.4	2.9	176.024	292.03	178.0
91.21	217.3	0.4198	26.004	22.4	498.5	6097.1602	10000	0.1223	0.01056	7621.5	7.6215E5	3.383E-3	0.4	3.0	177.004	279.82	173.8
85.26	209.7	0.4067	27.020	22.4	510.0	6303.3901	10000	0.1252	0.01160	7879.2	7.8792E5	3.384E-3	0.5	3.0	178.020	261.59	167.7
82.76	204.5	0.4046	28.004	22.4	488.6	6440.7100	10000	0.1199	0.01168	8050.9	8.0509E5	3.383E-3	0.5	3.0	179.004	253.90	163.6
78.67	199.3	0.3948	29.004	22.4	522.4	6578.0898	10000	0.1282	0.01316	8222.6	8.2226E5	3.384E-3	0.5	3.0	180.004	241.37	159.4
72.99	191.5	0.3812	30.000	22.4	529.1	6771.6001	10000	0.1299	0.01443	8464.5	8.4645E5	3.384E-3	0.5	3.0	181.000	223.92	153.2
70.59	186.4	0.3788	31.000	22.4	530.7	6896.3999	10000	0.1303	0.01528	8620.5	8.6205E5	3.384E-3	0.5	3.0	182.000	216.58	149.1
65.41	178.4	0.3666	32.008	22.4	543.1	7083.6499	10000	0.1333	0.01706	8854.6	8.8546E5	3.384E-3	0.5	3.1	183.008	200.68	142.7
62.17	173.1	0.3592	33.004	22.4	535.7	7202.0601	10000	0.1315	0.01788	9002.6	9.0026E5	3.384E-3	0.6	3.1	184.004	190.74	138.5
58.77	168.0	0.3499	34.004	22.4	543.9	7315.1499	10000	0.1335	0.01928	9143.9	9.1439E5	3.384E-3	0.6	3.1	185.004	180.32	134.4
54.34	160.0	0.3395	35.020	22.4	535.7	7482.7700	10000	0.1315	0.02092	9353.5	9.3535E5	3.383E-3	0.6	3.1	186.020	166.71	128.0
52.43	154.7	0.3390	36.020	22.4	546.4	7589.6401	10000	0.1341	0.02284	9487.1	9.4871E5	3.383E-3	0.6	3.1	187.020	160.85	123.7
49.44	149.6	0.3305	37.008	22.4	539.0	7688.4800	10000	0.1323	0.02408	9610.6	9.6106E5	3.383E-3	0.6	3.1	188.008	151.67	119.7
45.86	141.6	0.3238	38.020	22.4	543.9	7838.0098	10000	0.1335	0.02711	9797.5	9.7975E5	3.383E-3	0.6	3.2	189.020	140.71	113.3
42.12	136.3	0.3091	39.068	22.4	544.8	7931.4902	10000	0.1337	0.02933	9914.4	9.9144E5	3.383E-3	0.7	3.2	190.068	129.22	109.0
39.89	131.2	0.3040	40.008	22.4	565.4	8019.4102	10000	0.1388	0.03283	10024	1.0024E6	3.383E-3	0.7	3.2	191.008	122.39	105.0
36.04	123.3	0.2923	41.020	22.4	558.0	8149.2998	10000	0.1370	0.03671	10187	1.0187E6	3.383E-3	0.7	3.2	192.020	110.56	98.63
32.85	117.7	0.2791	42.004	22.4	567.1	8236.2197	10000	0.1392	0.04093	10295	1.0295E6	3.383E-3	0.7	3.2	193.004	100.77	94.17
30.54	112.5	0.2715	43.020	22.4	579.5	8310.8896	10000	0.1422	0.04580	10389	1.0389E6	3.383E-3	0.7	3.2	194.020	93.703	89.99
27.57	104.5	0.2638	44.004	22.4	568.7	8422.5898	10000	0.1396	0.05207	10528	1.0528E6	3.383E-3	0.7	3.3	195.004	84.576	83.60
24.96	98.85	0.2525	45.020	22.4	586.1	8497.0098	10000	0.1438	0.05999	10621	1.0621E6	3.384E-3	0.8	3.3	196.020	76.565	79.08
22.64	93.61	0.2418	46.004	22.4	575.3	8559.5303	10000	0.1412	0.06565	10699	1.0699E6	3.383E-3	0.8	3.3	197.004	69.448	74.89
19.46	85.58	0.2274	47.008	22.4	598.5	8652.1602	10000	0.1469	0.08171	10815	1.0815E6	3.383E-3	0.8	3.3	198.008	59.697	68.47
17.65	79.80	0.2212	48.004	22.4	592.7	8713.6602	10000	0.1455	0.09309	10892	1.0892E6	3.384E-3	0.8	3.3	199.004	54.158	63.84
15.46	74.53	0.2075	49.004	22.4	588.6	8763.1201	10000	0.1445	0.1060	10954	1.0954E6	3.384E-3	0.8	3.3	200.004	47.436	59.62
13.95	69.21	0.2015	50.004	22.4	582.0	8813.8604	10000	0.1428	0.1215	11017	1.1017E6	3.384E-3	0.8	3.4	201.004	42.786	55.37
11.76	63.46	0.1853	51.004	22.4	596.8	8861.7695	10000	0.1465	0.1482	11077	1.1077E6	3.383E-3	0.9	3.4	202.004	36.079	50.76
9.306	55.03	0.1691	52.004	22.4	597.7	8923.2002	10000	0.1467	0.1973	11154	1.1154E6	3.383E-3	0.9	3.4	203.004	28.550	44.03
7.803	49.59	0.1574	53.004	22.4	607.6	8959.9404	10000	0.1491	0.2471	11200	1.1200E6	3.384E-3	0.9	3.4	204.004	23.940	39.67
6.412	43.50	0.1474	54.004	22.4	599.3	8996.4102	10000	0.1471	0.3167	11246	1.1246E6	3.384E-3	0.9	3.4	205.004	19.671	34.80
4.835	37.13	0.1302	55.008	22.4	602.6	9026.7500	10000	0.1479	0.4372	11283	1.1283E6	3.384E-3	0.9	3.4	206.008	14.833	29.70
3.671	31.67	0.1159	56.004	22.4	600.2	9050.7803	10000	0.1473	0.5984	11313	1.1313E6	3.384E-3	0.9	3.5	207.004	11.264	25.33
2.529	25.16	0.1005	57.008	22.4	601.0	9074.4404	10000	0.1475	0.9494	11343	1.1343E6	3.383E-3	1.0	3.5	208.008	7.7578	20.13
1.433	17.90	0.08009	58.004	22.4	607.6	9091.7998	10000	0.1491	1.897	11365	1.1365E6	3.384E-3	1.0	3.5	209.004	4.3968	14.32
0.7208	11.89	0.06062	59.004	22.4	607.6	9103.0098	10000	0.1491	4.297	11379	1.1379E6	3.384E-3	1.0	3.5	210.004	2.2115	9.513
0.3527	7.680	0.04592	60.004	22.4	596.0	9107.7900	10000	0.1463	10.11	11385	1.1385E6	3.383E-3	1.0	3.5	211.004	1.0820	6.144

